Put a cup with a little D.D.T. in it just below the hole where they are going in and out. When the bee flys over the cup it will drop down into the powder and get it on it's body and then will bring it into the hive.
I which I still had a little of that stuff......it would kill anything. Put 1/2 teaspoon on a big ant hill..... and they are dead. The stuff that is sold now will only kill some of the ants and the rest just build a new nest a few feet away.
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